p-Toluenesulfonic acid → HCID 18770637, compound

HRID 2299060Notes

Reaction equation

HRID 2299060 reaction equation
[CH:1]1([C:7]([CH3:11])([CH3:10])[CH:8]=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:12][C:13]1[CH:21]=[CH:20][C:16]([C:17]([NH2:19])=[O:18])=[CH:15][CH:14]=1.[NH:22]1[C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=2[N:24]=[N:23]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:22]1([CH:8]([NH:19][C:17](=[O:18])[C:16]2[CH:20]=[CH:21][C:13]([Cl:12])=[CH:14][CH:15]=2)[C:7]([CH:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)([CH3:11])[CH3:10])[C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=2[N:24]=[N:23]1

Participants

5

Reactant 4

HCID 6101p-Toluenesulfonic acidHCID 120844-ChlorobenzamideHCID 1400235028523-30-0HCID 178418385HCID 178418385, compound

Product 1

HCID 18770637HCID 18770637, compound

Procedure

The product from Example 22A, 4-chlorobenzamide, benzotriazole, and p-toluenesulfonic acid were processed as described in Example 1C to provide the title compound.

Sources & evidence

ORD record
ord-b2e09283028e4896a638ae857b999934
Source dataset
uspto-grants-2002_12
Patent number
US06495576B2

Reaction notes

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