Benzamide → HCID 4421887, compound

HRID 2299076Notes

Reaction equation

HRID 2299076 reaction equation
[C:1]([NH2:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:10][C:11]([CH:14]=O)([CH3:13])[CH3:12].[NH:16]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[N:18]=[N:17]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:16]1([CH:14]([NH:9][C:1](=[O:8])[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[C:11]([CH3:12])([CH3:13])[CH3:10])[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[N:18]=[N:17]1

Participants

5

Reactant 4

HCID 2331BenzamideHCID 6101p-Toluenesulfonic acidHCID 12417PivalaldehydeHCID 178418385HCID 178418385, compound

Product 1

HCID 4421887HCID 4421887, compound

Procedure

A suspension of benzamide, pivaldehyde, benzotriazole, and p-toluenesulfonic acid was processed as in Example 1C to provide the title compound.

Sources & evidence

ORD record
ord-1d9f50d79f864c7e9b5be9c6356c41e2
Source dataset
uspto-grants-2002_12
Patent number
US06495576B2

Reaction notes

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