HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → N-[1-(1H-1,2,3-Benzotriazol-1-yl)-2,2-dimethylpropyl]-9-oxo-9H-fluorene-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Pivalaldehyde | HCID 12417 | — |
| Reactant | 9-Oxo-4-fluorenecarboxamide | HCID 297677 | — |
| Reactant | HCID 178418385 | HCID 178418385 | — |
| Product | N-[1-(1H-1,2,3-Benzotriazol-1-yl)-2,2-dimethylpropyl]-9-oxo-9H-fluorene-4-carboxamide | HCID 18379724 | — |
Reaction Steps
A suspension of the product from Example 68A, pivaldehyde, benzotriazole, and p-toluenesulfonic acid was processed as in Example 1C to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495576B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e09183b468a54b1481669107d43cd9e2 |
| Source note | uspto-grants-2002_12 |