p-Toluenesulfonic acid → HCID 18770563, compound

HRID 2299099Notes

Reaction equation

HRID 2299099 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[O:7])=[CH:4][CH:3]=1.[NH:11]1[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[N:13]=[N:12]1.[C:20]1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:11]1([CH2:20][NH:8][C:6](=[O:7])[C:5]2[CH:9]=[CH:10][C:2]([Cl:1])=[CH:3][CH:4]=2)[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[N:13]=[N:12]1

Participants

4

Reactant 3

HCID 6101p-Toluenesulfonic acidHCID 120844-ChlorobenzamideHCID 178418385HCID 178418385, compound

Product 1

HCID 18770563HCID 18770563, compound

Procedure

4-Chlorobenzamide, paraformaldehyede, benzotriazole, and p-toluenesulfonic acid were processed as described in Example 18B to provide the title compound.

Sources & evidence

ORD record
ord-a401a88da2a24286b666ce6682d0e33f
Source dataset
uspto-grants-2002_12
Patent number
US06495576B2

Reaction notes

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