HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3,4-dichlorophenyl)glycine → HCID 53814239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3,4-dichlorophenyl)glycine | HCID 351250 | — |
| Reactant | methyl (2S)-2-aminopentanoate hydrochloride | HCID 14118488 | — |
| Product | HCID 53814239 | HCID 53814239 | — |
Reaction Steps
Following General Procedure D and using N-(3,4-dichlorophenyl)glycine (from Example I above) and L-norvaline methyl ester hydrochloride (Sennchem), the title compound was prepared. The reaction was monitored by tlc (Rf=0.32 in 50% ethyl acetate/hexanes) and purification was by silica gel chromatography using ethyl acetate/hexanes as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495693B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-eaf20c55e66447139ce0eb0b70eb102a |
| Source note | uspto-grants-2002_12 |