HuagongsheHuagongshe Chemistry Print Report · For research reference only
Alanine methyl ester hydrochloride → HCID 54367074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| Reactant | HCID 15484845 | HCID 15484845 | — |
| Product | HCID 54367074 | HCID 54367074 | — |
Reaction Steps
Following General Procedure E and using L-alanine methyl ester hydrochloride (Sigma) and N-(3,5-difluorophenyl)-D,L-alanine (from Example C above), the title compound was prepared as a solid (mp=93-95° C.). The reaction was monitored by tlc (Rf=0.4 in 3% methanol/methylene chloride) and purification of this compound was by flash chromatography with 3% methanol/methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495693B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-d78a13f409a444d3a1a7a98dcf771f90 |
| Source note | uspto-grants-2002_12 |