HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl (benzylthio)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-((Phenylmethyl)thio)acetic acid | HCID 66897 | — |
| Product | Methyl (benzylthio)acetate | HCID 562502 | — |
Reaction Steps
S-benzylthioglycolic acid (12.0 g) was dissolved in 250 mL of methanol and sparged with hydrogen chloride gas at room temperature for 20 minutes. The solvent was then removed under vacuum. Methyl S-benzylthioglycolate obtained was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495719B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-468fb890d64e40a2a3924c8de2e5beb2 |
| Source note | uspto-grants-2002_12 |