HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (+)- → HCID 45486762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (+)- | HCID 643189 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 45486762 | HCID 45486762 | — |
Reaction Steps
2-methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with (R)-1-phenylethylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (CI): m/e 316.1 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.49 (br s, 1H); 8.37 (d, J=5.1 Hz, 1H); 7.83 (d, J=8.0 Hz, 1H); 7.3-7.5 (m, 8H); 6.77 (d, J=5.3 Hz, 1H); 6.03 (br s, 1H); 5.22 (br s, 1H); 1.65 (d, J=7.0 Hz, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-28a6aa9d76a9454c885374a10098e20d |
| Source note | uspto-grants-2002_12 |