2,3-Dichlorobenzylamine → HCID 18375922, compound

Participants

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 2,3-dichlorobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 370.1 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.58 (s, 1H); 8.44 (d, J=5.5 Hz, 1H); 7.93 (br s, 1H); 7.85 (d, J=8.3 Hz, 1H); 7.19 (t, J=5.8 Hz, 1H); 6.86 (d, J=5.5 Hz, 1H); 5.88 (br s, 1H); 4.86 (d, J=6.4 Hz, 2H).

Provenance & Evidence