HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cumylamine → HCID 17905808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cumylamine | HCID 68509 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 17905808 | HCID 17905808 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with cumylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 330.1 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.37 (d, J=4.8 Hz, 1H); 8.05 (br s, 1H); 7.77 (d, J=7.6 Hz; 1H); 7.54 (d, J=7.8 Hz, 2H); 7.41 (m, 2H); 6.75 (d, J=5.5 Hz; 1H); 5.91 (br s, 1H); 1.81 (s, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-d9aaf86dc7f64f17b14e056aeb5075b4 |
| Source note | uspto-grants-2002_12 |