HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzylamine → HCID 18375810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzylamine | HCID 81292 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375810 | HCID 18375810 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 2-methoxybenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 332.1 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.63 (s, 1H); 8.41 (br s, 1H); 8.12 (br s, 1H); 7.86 (m, 1H); 6.94 (m, 2H); 6.79 (d, J=5.2 Hz, 1H); 5.95 (br s, 1H); 4.74 (d, J=5.9 Hz, 2H); 3.92 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-46ca2d9a7e954fbd831b5eaf1b597f1f |
| Source note | uspto-grants-2002_12 |