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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300735Generated: October 30, 2026

3-Methoxybenzylamine → HCID 18375926, compound

https://huagongshe.com/reaction/2300735

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-MethoxybenzylamineHCID 21156—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 18375926HCID 18375926—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 3-methoxybenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. 1H NMR (500 MHz, CDCl3): δ 0.60 (br s, 1H); 8.44 (br s, 1H); 8.08 (br s, 1H); 7.86 (d, J=8.5 Hz, 1H); 7.3-7.5 (m, 3H); 7.02 (d, J=7.6 Hz; 1H); 6.98 (s, 1H); 6.85 (m, 2H); 5.86 (br s, 1H); 4.73 (d, J=5.7 Hz, 2H); 3.82 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-987791d92f21406f8d379e191d82f9ae
Source noteuspto-grants-2002_12