HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzylamine → HCID 18375885, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzylamine | HCID 67326 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375885 | HCID 18375885 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 4-fluorobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 320.1 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.60 (s, 1H); 8.43 (br s, 1H); 8.07 (br s, 1H); 7.86 (m, 1H); 7.38 (m, 5H); 7.07 (t, J=8.7 Hz, 1H); 6.85 (d, J=5.5 Hz, 1H); 5.79 (br s, 1H); 4.72 (d, J=5.7 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-0ad0d87eb658498aada1abdc82e388fb |
| Source note | uspto-grants-2002_12 |