HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzylamine → HCID 18375513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzylamine | HCID 66853 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375513 | HCID 18375513 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 3-fluorobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 320.2 (M+1). 1H NMR (500 MHz, CD3OD): δ partial 8.84 (br s, 1H); 8.39 (d, J=5.5 Hz, 1H); 7.97 (br s, 1H); 7.71 (d, J=8.2 Hz, 1H); 7.13 (d, J=10.1 Hz, 1H); 7.06 (d, J=5.5 Hz, 1H); 6.96 (m, 1H); 4.69 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-5b282cc9680348d48337cadeb3fd5680 |
| Source note | uspto-grants-2002_12 |