Benzenemethanamine, 3-bromo- → HCID 18375621, compound

Participants

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 3-bromobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 380.2, 382.2 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.58 (s, 1H); 8.44 (d, J=5.3 Hz, 1H); 8.01 (br s, 1H); 7.85 (m, 1H); 7.58 (s, 1H); 7.45 (d, J=7.5 Hz, 1H); 6.87 (d, J=5.5 Hz, 1H); 5.83 (br s, 1H); 4.74 (d, J=6.1 Hz, 2H).

Provenance & Evidence