3-Iodobenzylamine → HCID 18375844, compound

Participants

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 3-iodobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 428.1 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.59 (s, 1H); 8.44 (d, J=4.7 Hz, 1H); 8.02 (br s, 1H); 7.86 (m, 1H); 7.79 (s, 1H); 7.65 (d, J=7.8 Hz, 1H); 7.38 (m, 3H); 7.12 (t, J=7.8 Hz, 1H), 6.87 (d, J=5.3 Hz, 1H); 5.78 (br s, 1H); 4.71 (d, J=5.9 Hz, 2H).

Provenance & Evidence