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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300754Generated: October 30, 2026

4-Chlorobenzylamine → HCID 18375927, compound

https://huagongshe.com/reaction/2300754

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-ChlorobenzylamineHCID 66036—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 18375927HCID 18375927—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 4-chlorobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 336.0 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.59 (s, 1H); 8.43 (d, J=4.6 Hz, 1H); 8.02 (br s, 1H); 7.86 (m, 1H); 6.86 (d, J=5.5 Hz, 1H); 5.79 (br s, 1H ); 4.73 (d, J=5.9 Hz, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-2e87a20cbead4c43bb5f87ce27ed81d5
Source noteuspto-grants-2002_12