HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-phenylethan-1-ol → HCID 69963118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-phenylethan-1-ol | HCID 134797 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 69963118 | HCID 69963118 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with (S)-1-phenyl-2-hydroxyethylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (CI): m/e 332.2 (M+1). 1H NMR (500 Mz, CD3OD): δ partial 8.58 (br s, 1H); 8.38 (s, 1H); 7.69 (d, J=7.3 Hz, 1H); 7.47 (d, J=7.3 Hz, 2H); 7.02 (d, J=5.5 Hz, 1H); 5.16 (s, 1H); 3.81-3.91 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a4d275f265d941a8ae7ecfe3843f62a0 |
| Source note | uspto-grants-2002_12 |