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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300757Generated: November 1, 2026

2-Amino-2-phenylethan-1-ol → HCID 69963118, compound

https://huagongshe.com/reaction/2300757

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Amino-2-phenylethan-1-olHCID 134797—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 69963118HCID 69963118—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with (S)-1-phenyl-2-hydroxyethylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (CI): m/e 332.2 (M+1). 1H NMR (500 Mz, CD3OD): δ partial 8.58 (br s, 1H); 8.38 (s, 1H); 7.69 (d, J=7.3 Hz, 1H); 7.47 (d, J=7.3 Hz, 2H); 7.02 (d, J=5.5 Hz, 1H); 5.16 (s, 1H); 3.81-3.91 (m, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-a4d275f265d941a8ae7ecfe3843f62a0
Source noteuspto-grants-2002_12