Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300761Generated: October 31, 2026

(S)-(+)-1-Cyclohexylethylamine → HCID 45486772, compound

https://huagongshe.com/reaction/2300761

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(S)-(+)-1-CyclohexylethylamineHCID 5325951—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 45486772HCID 45486772—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with (S)-1-cyclohexylethylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): 322.3 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.63 (s, 1H); 8.30 (br s, 1H); 8.23 (br s, 1H); 7.88 (d, J=7.3 Hz, 1H); 7.43 (m, 2H); 6.80 (d, J=5.2 Hz, 1H); 4.10 (m, 1H); 1.69-1.91 (m, 4H); 1.10-1.35 (m, 10H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-118d7cc506734b01a6577068aa2fb53f
Source noteuspto-grants-2002_12