Water → HCID 18377467, compound

Participants

Reaction Steps

A mixture of 4.48 g (0.020 mole) of 2-bromo-6-methylpyridine hydrochloride, 3.34 g (0.022 mole) of 2,5-dimethylbenzylmercaptan and 0.88 g (0.022 mole) of powdered sodium hydroxide were stirred together at room temperature in 35 ml of DMF for 3.5 hours. The reaction mixture was poured into water and the precipitate filtered off and washed with water. Yield 1.96 g or 38%.

Provenance & Evidence