HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300993Generated: October 30, 2026
1-Methyl-2(1H)-pyridinethione → HCID 10192947, compound
https://huagongshe.com/reaction/2300993
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Methyl-2(1H)-pyridinethione | HCID 16277 | — |
| Reactant | Benzene, 2-(chloromethyl)-1,4-dimethyl- | HCID 69987 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10192947 | HCID 10192947 | — |
Reaction Steps
A mixture of 5.0 g of 1-methyl-2(1H)-pyridinethione and 6.2 g of 2,5-dimethylbenzyl-chloride in 40 ml of toluene was heated for five hours at 70° C. A pale yellow solid was filtered from the cooled mixture. Yield was 5 g having a melting point of 130-137° C. NMR and infrared spectra were consistent with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06498254B1 |
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| Source dataset | uspto-grants-2002_12 |
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| ORD ID | ord-656b2a20a9224861a9cd97145866e476 |
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| Source note | uspto-grants-2002_12 |
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