HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-t-Butoxycarbonyl-2-methyl-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine → HCID 18377285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-t-Butoxycarbonyl-2-methyl-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine | HCID 18377356 | — |
| Solvent | Hydrochloride methanol | HCID 21893726 | — |
| Product | HCID 18377285 | HCID 18377285 | — |
Reaction Steps
5-t-Butoxycarbonyl-2-methyl-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine (100 mg, 0.40 mmol) was dissolved in hydrochloric acid methanol solution and stirred at room temperature for 14 hours. By evaporating the solvent from the reaction solution under a reduced pressure, 60 mg (0.39 mmol, 99% in yield) of the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498251B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-82b6666a51ef471583929e28647909ce |
| Source note | uspto-grants-2002_12 |