Ethylmorpholine → HCID 18371944, compound

Participants

Reaction Steps

The procedure according to Example 1, 253 g (2.2 mol) of 4-ethylmorpholine was added dropwise to 144 g (2 mol) of trimethylaluminum under nitrogen gas flow with stirring. The resulting mixture was stirred for 6 hours at room temperature for reaction completion, and then the mixture was dried under vacuum at 65° C. and distilled under vacuum at 90° C. to give 329 g of the colorless 4-ethylmorpholine trimethylaluminum having high purity.

Provenance & Evidence