Ethylmorpholine → HCID 18371944, compound

HRID 2301214Notes

Reaction equation

HRID 2301214 reaction equation
[CH2:1]([N:3]1[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1)[CH3:2].[CH3:9][Al:10]([CH3:12])[CH3:11]>>[CH3:9][Al:10]([CH3:12])[CH3:11].[CH2:1]([N:3]1[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1)[CH3:2]

Participants

3

Reactant 2

HCID 7525EthylmorpholineHCID 16682925Trimethylaluminum

Product 1

HCID 18371944HCID 18371944, compoundYield 87.8%

Procedure

The procedure according to Example 1, 253 g (2.2 mol) of 4-ethylmorpholine was added dropwise to 144 g (2 mol) of trimethylaluminum under nitrogen gas flow with stirring. The resulting mixture was stirred for 6 hours at room temperature for reaction completion, and then the mixture was dried under vacuum at 65° C. and distilled under vacuum at 90° C. to give 329 g of the colorless 4-ethylmorpholine trimethylaluminum having high purity.

Workup

  1. stirringThe resulting mixture was stirred for 6 hours at room temperature for reaction completion
  2. customthe mixture was dried under vacuum at 65° C.
  3. distillationdistilled under vacuum at 90° C.

Sources & evidence

ORD record
ord-ca5d032639e34123b8a69450dee49b97
Source dataset
uspto-grants-2002_12
Patent number
US06500250B1

Reaction notes

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