HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 3-nitro- → 3-Nitro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 3-nitro- | HCID 8495 | — |
| Reactant | 3-amino-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)benzamide | HCID 18372001 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 3-Nitro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)benzamide | HCID 18372011 | — |
Reaction Steps
3-Nitro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)benzamide was prepared by reaction of 3-nitrobenzoylchloride with VIII as in scheme A (above), then converted to 3-amino-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)benzamide by catalytic hydrogenation using palladium as the catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500405B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-744720d810bc49e3b0cfe6af3a16f0de |
| Source note | uspto-grants-2002_12 |