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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2301271Generated: October 30, 2026

Benzene, 1-ethoxy-4-isocyanato- → HCID 9889519, compound

https://huagongshe.com/reaction/2301271

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, 1-ethoxy-4-isocyanato-HCID 122887—
ReactantHCID 11357928HCID 11357928—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 9889519HCID 9889519—

Reaction Steps

1.0 g (3.59 mmol) of 2-{[2-dimethylaminoethyl]amino}-N,4-dimethyl-1,3-thiazole-5-sulphonamide and 586 mg (3.59 mmol) of 4-ethoxyphenyl isocyanate are dissolved in 30 ml of dioxane and stirred at room temperature for 12 h. The mixture is then concentrated in vacuo, and the residue is recrystallized from 2-propanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06500817B1
Source datasetuspto-grants-2002_12
ORD IDord-6c6e235a7851477ba1ee63fd8d627343
Source noteuspto-grants-2002_12