HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-ethoxy-4-isocyanato- → HCID 9889519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-ethoxy-4-isocyanato- | HCID 122887 | — |
| Reactant | HCID 11357928 | HCID 11357928 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 9889519 | HCID 9889519 | — |
Reaction Steps
1.0 g (3.59 mmol) of 2-{[2-dimethylaminoethyl]amino}-N,4-dimethyl-1,3-thiazole-5-sulphonamide and 586 mg (3.59 mmol) of 4-ethoxyphenyl isocyanate are dissolved in 30 ml of dioxane and stirred at room temperature for 12 h. The mixture is then concentrated in vacuo, and the residue is recrystallized from 2-propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500817B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-6c6e235a7851477ba1ee63fd8d627343 |
| Source note | uspto-grants-2002_12 |