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HRID2301273

反应详情

EQUATION

反应方程式

HRID 2301273 的结构方程式

REACTANTS

反应物

1
结构：C=CCOC(=O)N[C@@H](Cc1ccc(C(=N)N)cc1)C(=O)OCC.Cl
HCID70002038

未命名化合物

PRODUCTS

生成物

1
结构：C=CCOC(=O)N[C@@H](Cc1ccc(C(=N)N)cc1)C(=O)O.Cl
HCID68613816

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

17 g (0.048 mol) of (S)-2-allyloxycarbonylamino-3-(4-carbamimidoylphenyl)propionic acid ethyl ester hydrochloride were treated with 400 ml of half-concentrated hydrochloric acid for 3 h at RT. The solvent was evaporated (<30° C.) and the residue was stirred with ether. Yield=15 g (95%). MS=292.2 (M+1)+.

WORKUP

后处理

  1. customThe solvent was evaporated (<30° C.)