HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 18372613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 18372489 | HCID 18372489 | — |
| Product | HCID 18372613 | HCID 18372613 | — |
Reaction Steps
The title compound is prepared from 5-chloro-N-(4-chlorophenyl)-8-methoxy-7-quinolinesulfonamide, which is the first title compound of Preparation 9, and 6 equivalents of BBr3 according to the procedure described in Example 18. Crystallization from Et2O/hexane/CH2Cl2 affords 0.015 g of the title compound as a red-brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500842B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-60aadbccc3f64c46beeca926c6f8b13c |
| Source note | uspto-grants-2002_12 |