HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 18372559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 18372710 | HCID 18372710 | — |
| Product | HCID 18372559 | HCID 18372559 | — |
Reaction Steps
The title compound is prepared from 5-chloro-8-methoxy-N-(3-phenylpropyl)-7-quinolinesulfonamide, which is the title compound of Preparation 11, and 6 equivalents of BBr3 according to the procedure described in Example 18. Crystallization from CHCl3/acetone/EtOH affords 0.063 g of the title compound as a red-brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500842B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e1ca4ac2fac14a108f997656ad727abc |
| Source note | uspto-grants-2002_12 |