HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 11612085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 3-Amino-6-chloro-2-hydroxy-benzenesulfonamide | HCID 11368059 | — |
| Reactant | 1-(Benzyloxy)-2-isocyanatobenzene | HCID 18373464 | — |
| Product | HCID 11612085 | HCID 11612085 | 26.3% |
Reaction Steps
Following the general procedure for urea formation outlined in example 12, 3-amino-6-chloro-2-hydroxybenzenesulfonamide (52 mg, 0.23 mmol) and 2-benzyloxyphenylisocyanate (40 mg, 0.17 mmol) were coupled to form the desired urea (20 mg, 26%). EI-MS (m/z) 446.2, 448.3, 450.2 (M−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a6b8d3a491644accaa109156c2a26cf0 |
| Source note | uspto-grants-2002_12 |