HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18373447, compound → HCID 18373556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18373447 | HCID 18373447 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18373556 | HCID 18373556 | 95% |
Reaction Steps
Following the general hydrogenation procedure outlined in example 15, 6-chloro-2-hydroxy-1-(4-morpholinylsulfonyl)-3-nitrobenzene (210 mg, 0.65 mmol) was reduced with hydrogen and Pd/C (100 mg) to form the desired product (180 mg, 95%). 1H NMR (MeOD-d4): δ 6.28 (mn, 2H), 3.68 (t, 4H), 3.30 (t, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-0306ec6f92c141a89d31fc243dc2e895 |
| Source note | uspto-grants-2002_12 |