HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54395400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Reactant | 2,6-Dichloro-3-nitrobenzene-1-sulfonyl chloride | HCID 23447772 | — |
| Product | HCID 54395400 | HCID 54395400 | 75% |
Reaction Steps
Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (600 mg, 2.07 mmol), 4-(2-aminoethyl) morpholine (269 mg, 2.07 mmol) and triethylamine (0.58mL, 4.13 mmol) were reacted to form the desired product (593 mg, 75%). LC-MS (m/z) 384.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-ad86de335f724b03966fb9a48fb01887 |
| Source note | uspto-grants-2002_12 |