HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 11541835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 11534542 | HCID 11534542 | — |
| Product | HCID 11541835 | HCID 11541835 | 44% |
Reaction Steps
Following the general procedure for Boc deprotection outlined in example 36, N-[3-[N″-[(1-tert-butoxycarbonylpiperidin4-yl)methyl]aminosulfonyl]-4-chloro-2-hydroxyphenyl]-N′-(2,3-dichlorophenyl) urea (20 mg, 0.033 mmol) was stirred in trifluoroacetic acid to form the desired product (9 mg, 44%). LC-MS (m/z) 509.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-5c79a9644e374247b938d99f9366e593 |
| Source note | uspto-grants-2002_12 |