HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18373532, compound → HCID 18373537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18373532 | HCID 18373532 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18373537 | HCID 18373537 | 95% |
Reaction Steps
Following the general hydrogenation procedure outlined in example 15, 6-chloro-2-hydroxy-3-nitro- 1-(1-oxidothiomorpholinosulfonyl)benzene (103 mg, 0.29mmol) was reduced with hydrogen and 10% Pd/C (59 mg) to form the desired product (89 mg, 95%). LC-MS (m/z) 325.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-8970bcc9d7744a93be9d209d604faf67 |
| Source note | uspto-grants-2002_12 |