HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 9914720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | HCID 18373537 | HCID 18373537 | — |
| Product | HCID 9914720 | HCID 9914720 | 46% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, 4-chloro-2-hydroxy-3-(1-oxidothiomorpholinosulfonyl)aniline (88 mg, 0.27 mmol) and 2-bromophenylisocyanate (65 mg, 0.33 mmol) were coupled to form the desired urea (65 mg, 46%). LC-MS (m/z) 524.2 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-8bb30385193c4eaba5b3d9ed1a7d3bcf |
| Source note | uspto-grants-2002_12 |