Triethylamine → HCID 17927860, compound

Participants

Reaction Steps

Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (1.0 g, 3.44 mmol), azetidine hydrochloride (320 mg, 3.44 mmol) and triethylamine(1.44mL, 10.32 mmol) were reacted to form the desired product (510 mg, 48%). 1H NMR (MeOD-d4): δ 7.94 (d, 1H), 7.79 (d, 1H), 4.16 (t, 4H), 2.29 (m, 2H).

Provenance & Evidence