Triethylamine → HCID 17927831, compound

Participants

Reaction Steps

Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (1.39 g, 4.78 mmol), cyclopropylamine (273 mg, 4.78 mmol) and triethylamine(1.0 mL, 7.17 mmol) were reacted to form the desired product (1.15 g, 77%). 1H NMR (MeOD-d4): δ 7.72 (d, 1H), 7.65 (d, 1H), 2.34 (m, 1H), 0.75 (m, 4H).

Provenance & Evidence