Water → HCID 18373507, compound

Participants

Reaction Steps

Following the general hydrolysis procedure outlined in example 15, N-cyclopropyl-2,6-dichloro-3-nitrobenzenesulfonamide (1.15 g, 3.70 mmol), 60% NaH (444 mg, 11.1 mmol) and water (67 μL, 3.70 mmol) were reacted to form the desired product (740 mg, 68%). 1H NMR (MeOD-d4): δ 8.06 (d, 1H), 7.24 (d, 1H), 2.29 (m, 1H), 0.60 (m, 4H).

Provenance & Evidence