HCID 18373507, compound → HCID 18373462, compound

Participants

Reaction Steps

Following the general hydrogenation procedure outlined in example 15, N-cyclopropyl-6-chloro-2-hydroxy-3-nitrobenzenesulfonamide (740 mg, 2.53 mmol) was reduced with hydrogen and 10% Pd/C (350 mg) to form the desired product (660 mg, 99%). 1H NMR (MeOD-d4): δ 6.83 (m, 2H), 2.20 (m, 1H), 0.56 (m, 4H).

Provenance & Evidence