Propylamine → HCID 17927876, compound

Participants

Reaction Steps

Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (1.3 g, 4.48 mmol), propylamine (264 mg, 4.48 mmol) and triethylamine(0.94mL, 6.72 mmol) were reacted to form the desired product (10 g, 71%). 1H NMR (MeOD-d4): δ7.92 (d, 1H), 7.78 (d, 1H), 3.00 (t, 2H), 1.50 (m, 2H), 0.88 (t, 3H).

Provenance & Evidence