HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18373450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 17927876 | HCID 17927876 | — |
| Product | HCID 18373450 | HCID 18373450 | 69.1% |
Reaction Steps
Following the general hydrolysis procedure outlined in example 15, N-propyl-2,6-dichloro-3-nitrobenzenesulfonamide (1.0 , 3.19mmol), 60% NaH (393 mg, 3.19 mmol) and water (58 μL, 3.19 mmol) were reacted to form the desired product (650 mg, 69%). LC-MS (m/z) 295.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-fca6f124d60a4f45b85a6937e2a9e594 |
| Source note | uspto-grants-2002_12 |