HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 11719404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 1,2-Dichloro-3-isocyanatobenzene | HCID 33050 | — |
| Reactant | HCID 18373574 | HCID 18373574 | — |
| Product | HCID 11719404 | HCID 11719404 | 81% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, N-propyl-3-amino-6-chloro-2-hydroxybenzenesulfonamide (186 mg, 0.71 mmol) and 2,3-dichlorophenylisocyanate (133 mg, 0.71 mmol) were coupled to form the desired urea (259 mg, 81%). LC-MS (m/z) 452.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-bee663c2e5924684a67a25dbd6c94ec0 |
| Source note | uspto-grants-2002_12 |