Water → HCID 18373485, compound

Participants

Reaction Steps

Following the general hydrolysis procedure outlined in example 15, N-ethyl-2,6dichloro-3-nitrobenzenesulfonamide (1.16 g, 3.88mmol), 60% NaH (466 mg, 11.64 mmol) and water (70 μL, 3.88 mmol) were reacted. The crude product (1.34 g) was carried on to the next step without purification. 1H NMR (MeOD-d4): δ 8.07 (d, 1H), 7.25 (d, 1H), 3.05 (q, 2H), 1.12 (t, 3H).

Provenance & Evidence