HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18373541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18373440 | HCID 18373440 | — |
| Product | HCID 18373541 | HCID 18373541 | 77% |
Reaction Steps
Following the general hydrolysis procedure outlined in example 15, N-(2-benzyloxyethyl)-2,6-dichloro-3-nitrobenzenesulfonamide (2.31 g, 5.71 mmol), 60% NaH (683 mg, 17.1mmol) and water (103 μ, 5.72mmol) were reacted to form the desired product (1.70 g, 77%). LC-MS (m/z) 387.5(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-eadedfba51b549edabd6ff8752fc0ecb |
| Source note | uspto-grants-2002_12 |