HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 17927791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | (Cyclopropylmethyl)ammonium chloride | HCID 81671 | — |
| Reactant | 2,6-Dichloro-3-nitrobenzene-1-sulfonyl chloride | HCID 23447772 | — |
| Product | HCID 17927791 | HCID 17927791 | 84% |
Reaction Steps
Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (1.5 g, 5.2 mmol), aminomethyl cyclopropane hydrochloride (0.56 g, 5.2 mmol) and triethylamine (1.8mL, 12.9 mmol) were reacted to form the desired product (1.28 g, 84%). LC-MS m/z 325 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-bc834d51dab8452c9e19a0f8bdb2e92d |
| Source note | uspto-grants-2002_12 |