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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2301607Generated: October 28, 2026

Water → HCID 18373547, compound

https://huagongshe.com/reaction/2301607

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium hydrideHCID 24758—
ReactantHCID 17927791HCID 17927791—
ProductHCID 18373547HCID 1837354772.7%

Reaction Steps

Following the general hydrolysis procedure outlined in example 15, N-cyclopropylmethyl-2,6 dichloro-3-nitrobenzenesulfonamide (0.85 g, 2.6 mmol), 80% NaH (0.23 g, 9.88 mmol) and water (56 μL, 3.1 mmol) were reacted to form the desired product (0.58 g, 72%). LC-MS m/z 307 M+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06500863B1
Source datasetuspto-grants-2002_12
ORD IDord-505b7d0afe4847c18c1cd6ccd9c91d69
Source noteuspto-grants-2002_12