HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 11662688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 1,2-Dichloro-3-isocyanatobenzene | HCID 33050 | — |
| Reactant | HCID 18373511 | HCID 18373511 | — |
| Product | HCID 11662688 | HCID 11662688 | 53.8% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, 3-amino-6-chloro-N-cyclopropylmethyl-2-hydroxybenzenesulfonamide (0.23 g, 0.77mmol) and 2,3-dichlorophenylisocyanate (100 μL, 0.76 mmol) were coupled to form the desired urea (0.19 g, 53%). LC-MS m/z 464 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a13684a1c844401da5e3cf9f24cccb32 |
| Source note | uspto-grants-2002_12 |