HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86588373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2,6-Dichloro-3-nitrobenzene-1-sulfonyl chloride | HCID 23447772 | — |
| Product | HCID 86588373 | HCID 86588373 | 68% |
Reaction Steps
Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (151 g, 5.2 mmol), pyrrolidine (435 μL, 5.2 mmol) and triethylamine(1.1 mL, 7.8 mmol) were reacted to form the desired product (1.16 g, 68%). LC-MS m/z 325(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-5a5db6db83b84164a6f95d78da205359 |
| Source note | uspto-grants-2002_12 |