HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86588374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 86588373 | HCID 86588373 | — |
| Product | HCID 86588374 | HCID 86588374 | 85.9% |
Reaction Steps
Following the general hydrolysis procedure outlined in example 15, (N-pyrrolidinyl)-2,6 dichloro-3-nitrobenzenesulfonamide (1.12 g, 3.4mmol), 80% NaH (0.31 g, 10.3 mmol) and water (74 μL, 4.1mmol) were reacted to form the desired product (0.94 g, 69%). LC-MS m/z 307(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-67f0141eb946495099356be158607fd8 |
| Source note | uspto-grants-2002_12 |