HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminopyridine → HCID 18373479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminopyridine | HCID 1727 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Dichloro-3-nitrobenzene-1-sulfonyl chloride | HCID 23447772 | — |
| Product | HCID 18373479 | HCID 18373479 | 76% |
Reaction Steps
Following the general procedure for sulfonamide formation outlined in example 15, 2,6-dichloro-3-nitrobenzenesulfonyl chloride (500 mg, 1.72 mmol), 4-aminopyridine (165 mg,1.75 mmol) and triethylamine (0.36mL,2.58 mmol) were reacted to form the desired product (446 mg, 76%). EI-MS m/z 346(M-H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-248108dc7ab04ba0bd11116b775dbfa6 |
| Source note | uspto-grants-2002_12 |